HRID1598256

反应详情

EQUATION

反应方程式

HRID 1598256 的结构方程式

PROCEDURE

实验过程

As described for Example 8, 0.500 g of 10,11-dihydro-10-(4-aminobenzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine is reacted with 0.267 g of tetrahydrofurane-2-carbonyl chloride to give a glass which is crystallized from ethyl acetate to give 0.22 g of crystals, m.p. 208°-214° C.

WORKUP

后处理

  1. customto give a glass which
  2. customis crystallized from ethyl acetate