HCID 416666, compound → HCID 18933579, compound

HRID 1598323Notes

Reaction equation

HRID 1598323 reaction equation
[OH:1][C:2]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[CH:4][C:3]=1[CH2:10][N:11]([CH3:13])[CH3:12].[Cl:14][C:15]1[CH:26]=[CH:25][C:18]([CH2:19][N:20]([CH3:24])[CH2:21][CH2:22]O)=[CH:17][CH:16]=1>>[Cl:14][C:15]1[CH:16]=[CH:17][C:18]([CH2:19][N:20]([CH2:21][CH2:22][O:1][C:2]2[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[CH:4][C:3]=2[CH2:10][N:11]([CH3:13])[CH3:12])[CH3:24])=[CH:25][CH:26]=1

Participants

3

Reactant 2

HCID 416666HCID 416666, compoundHCID 10419703HCID 10419703, compound

Product 1

HCID 18933579HCID 18933579, compound

Procedure

The title compound (b.p. 100° C. at 0.1 mbar) was prepared by reacting 4-hydroxy-3-(dimethylaminomethyl)benzonitrile (7.32 g) with N-(4-chlorobenzyl)-N-methylethanolamine (8.29 g) in a similar manner to Example 4.

Sources & evidence

ORD record
ord-b045f6b584c74944acd00094d58e314f
Source dataset
uspto-grants-1998_04
Patent number
US05736568

Reaction notes

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