HRID1598395

反应详情

EQUATION

反应方程式

HRID 1598395 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

32.9 g of 4-(tert.butyloxycarbonylmethyloxy)-4'-cyano-biphenyl dissolved in 250 ml of methylene chloride is mixed slowly with 137 ml of trifluoroacetic acid. After stirring for 3 hours, the reaction mixture is evaporated to dryness and the solid residue is triturated with water.

WORKUP

后处理

  1. customthe reaction mixture is evaporated to dryness
  2. customthe solid residue is triturated with water