Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methoxy-6-nitrobenzoic acid → 2-Amino-6-methoxybenzoic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methoxy-6-nitrobenzoic acid | HCID 13300035 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Amino-6-methoxybenzoic Acid | HCID 2735357 | 100.2% |
반응 단계
A solution of 6-methoxy-2-nitrobenzoic acid (3.25 g, 16.5 mM) in ethanol (180 mL) containing 10% palladium-on-carbon catalyst (0.30 g) was hydrogenated using a Parr apparatus. When hydrogen consumption ceased, the resulting mixture was filtered through diatomaceous earth and the filtrate concentrated to provide the title benzoic acid (2.76 g, 100%) as a tan solid; MS(CI): 168 (M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05739133 |
| 출처 데이터셋 | uspto-grants-1998_04 |
| ORD ID | ord-0b896b1fc36047c1b419373f25b98e8f |
| 출처 메모 | uspto-grants-1998_04 |