Deferoxamine → Deferoxamine

HRID 1598822Notes

Reaction equation

HRID 1598822 reaction equation
[CH2:1]([S:9]([OH:12])(=[O:11])=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH3:13][C:14]([N:16]([OH:51])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][NH:22][C:23]([CH2:25][CH2:26][C:27]([N:29]([OH:50])[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][NH:35][C:36]([CH2:38][CH2:39][C:40]([N:42]([OH:49])[CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][NH2:48])=[O:41])=[O:37])=[O:28])=[O:24])=[O:15]>>[CH2:1]([S:9]([O-:12])(=[O:10])=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH3:13][C:14]([N:16]([OH:51])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][NH:22][C:23]([CH2:25][CH2:26][C:27]([N:29]([OH:50])[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][NH:35][C:36]([CH2:38][CH2:39][C:40]([N:42]([OH:49])[CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][NH2:48])=[O:41])=[O:37])=[O:28])=[O:24])=[O:15]

Participants

4

Reactant 2

HCID 2973DeferoxamineHCID 499391-Octanesulfonic acid

Product 2

HCID 2973DeferoxamineHCID 35715191-Octanesulfonate

Procedure

Following a procedure analogous to that of Example 1, octane-1-sulphonic acid and desferrioxamine-B are reacted to give the octane-1-sulphonate salt of desferrioxamine-B. Mp 144° C. C33H66O11 N6S Calcd C: 52.50%, H:8.81%, N:11.13%, S:4.25%; Found C: 52.43%, H:8.75%, N:11.16%, S:4.18%.

Workup

  1. customare reacted

Sources & evidence

ORD record
ord-b954d89565ed45e1ab8164ab1d4e7fab
Source dataset
uspto-grants-1998_04
Patent number
US05739167

Reaction notes

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