HRID1598823

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(=O)N(O)CCCCCNC(=O)CCC(=O)N(O)CCCCCNC(=O)CCC(=O)N(O)CCCCCN

HCID2973

Deferoxamine

C25H48N6O8

HCID15192

1-Dodecanesulfonic acid

C12H26O3S

PRODUCTS

生成物

HCID2973

Deferoxamine

C25H48N6O8

HCID3383616

1-Dodecanesulfonic acid, ion(1-)

C12H25O3S-

PROCEDURE

实验过程

Following a procedure analogous to that of Example 1, dodecane-1-sulphonic acid and desferrioxamine-B are reacted to give the dodecane-1-sulphonate salt of desferrioxamine-B, Mp 151° C. C37H74O11 N6S Calcd C: 54.79%, H:9.20%, N:10.36%, S:3.95%; Found C: 54.74%, H: 9.15%, N:10.21%, S: 4.07%.

WORKUP

后处理

customare reacted

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-48c91916181349579ad930d8838916f3
来源数据集: uspto-grants-1998_04
DOI: 10.6084/m9.figshare.5104873.v1
专利: US05739167
来源说明: uspto-grants-1998_04

反应 SMILES

[CH2:1]([S:13]([OH:16])(=[O:15])=[O:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH3:17][C:18]([N:20]([OH:55])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][NH:26][C:27]([CH2:29][CH2:30][C:31]([N:33]([OH:54])[CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][NH:39][C:40]([CH2:42][CH2:43][C:44]([N:46]([OH:53])[CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][NH2:52])=[O:45])=[O:41])=[O:32])=[O:28])=[O:19]>>[CH2:1]([S:13]([O-:16])(=[O:14])=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH3:17][C:18]([N:20]([OH:55])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][NH:26][C:27]([CH2:29][CH2:30][C:31]([N:33]([OH:54])[CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][NH:39][C:40]([CH2:42][CH2:43][C:44]([N:46]([OH:53])[CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][NH2:52])=[O:45])=[O:41])=[O:32])=[O:28])=[O:19]