Benzyl Benzoate → HCID 86752395, compound

Participants

Reaction Steps

Hy method A [Lawesson's reagent]. Benzyl benzoate (2.1 g) was heated at 140° C. for 24 h with Lawesson's Reagent (4.9 g) in anhydrous xylene (10 ml). After removal of the solvent and subjection of the mixture to chromatography on silica gel and recrystallization from pentane at low temperature, benzyl thionobenzoate was obtained in 67% yield. 1H NMR (CDCl3): δ=5.64 (s, 2H), 7.3-8.2 (m, 10H).

Provenance & Evidence