HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 15525522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | (2-Hydroxyphenyl)acetic acid | HCID 11970 | — |
| Solvent | Benzyl Alcohol | HCID 244 | — |
| Product | HCID 15525522 | HCID 15525522 | 4,264.7% |
Reaction Steps
A suspension of 22.6 g of 2-hydroxyphenylacetic acid, 0.5 g of paratoluenesulphonic acid in 15.5 cm3 of benzyl alcohol is heated at reflux for three hours. 2 g of 3S active carbon are added, the suspension is filtered over Supercel, and the filtrate is evaporated to dryness under reduced pressure (2.7 kPa). 30 g of benzyl [(2-hydroxy)phenyl]acetate are obtained in the form of crystals. M.p.K =104° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05739351 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-3dbd89ac72a94dfc90f70f116fb03c62 |
| Source note | uspto-grants-1998_04 |