HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 18931753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 2-[(propan-2-ylideneamino)oxy]butan-1-ol | HCID 270560 | — |
| Reactant | HCID 18931757 | HCID 18931757 | — |
| Product | HCID 18931753 | HCID 18931753 | 50% |
Reaction Steps
The starting material was a mixture of 2-propanone O-(2-hydroxybutyl)oxime and 2-propanone O-(2-hydroxy-1-ethylethyl)oxime in the ratio 96.7:3.3. Phenol was used in place of 4-chlorophenol, otherwise the procedure was as in Example 1. This resulted in O-(2-phenoxybutyl)hydroxylamine (yield: 50%) and O-(2-phenoxy-1-ethylethyl)hydroxylamine in the ratio 99.8:0.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05739402 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-450045f8b716414ba2b6f7c896ccecad |
| Source note | uspto-grants-1998_04 |