HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(N-ethyl-m-toluidino)ethanol → 2-(N-Ethyl-m-toluidino)ethyl benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(N-ethyl-m-toluidino)ethanol | HCID 7067 | — |
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 2-(N-Ethyl-m-toluidino)ethyl benzoate | HCID 3016260 | — |
Reaction Steps
Benzoylchloride (3.3 g) was added to a mixture of N-ethyl-N-hydroxyethyl-3-methylaniline (2.1 g) in acetone (25 cm3) and pyridine (1 cm3) and stirred at reflux for 1 hour. The reaction mixture was cooled and used directly in iv) below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05739299 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-8bb22e8b3b4743d79c25ce656d2612d5 |
| Source note | uspto-grants-1998_04 |