1-Methoxy-2-propanol → HCID 18931651, compound
Reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([CH2:16][CH2:17][C:18]([O:20][CH3:21])=[O:19])[CH:8]=[C:9]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:10]=1[OH:11])([CH3:4])([CH3:3])[CH3:2].[CH3:22][O:23][CH2:24][CH:25](O)C>>[C:1]([C:5]1[CH:6]=[C:7]([CH2:16][CH2:17][C:18]([O:20][CH2:21][CH:24]([O:23][CH3:22])[CH3:25])=[O:19])[CH:8]=[C:9]([C:12]([CH3:13])([CH3:14])[CH3:15])[C:10]=1[OH:11])([CH3:2])([CH3:3])[CH3:4]Participants
3
Procedure
The title compound was prepared from methyl 3-(3,5-di-t-butyl-4-hydroxyphenyl)propionate and propylene glycol monomethyl ether, by a procedure analogous to that of Reference Example 10. White powder with mellting point 73°-74° C.
Workup
- customwith mellting point 73°-74° C.
Sources & evidence
- ORD record
- ord-7b37b981569a43c68e50e76d9c0e806a
- Source dataset
- uspto-grants-1998_04
- Patent number
- US05739377
Reaction notes
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