Chromium oxide → Bismuth oxide antimony oxide chromium oxide boron oxide

HRID 1599355Notes

Reaction equation

HRID 1599355 reaction equation
[Bi:1]=[O:2].[Sb:3]=[O:4].[O-2:5].[Cr+3:6].[O-2].[O-2].[Cr+3].[B:10]=O>>[Bi:1]=[O:2].[Sb:3]=[O:4].[O-2:2].[Cr+3:6].[O-2:2].[O-2:2].[Cr+3:6].[B:10]=[O:5]

Participants

5

Procedure

A bismuth oxide powder (whose average particle size is about 2 to 3 μm), an antimony oxide fine powder (whose average particle size is about 2 to 3 μm), and a chromium oxide powder (whose average particle size is about 0.5 to 1.5 μm) were mixed at a weight ratio of 85:10:5. The mixed powder was heat treated at a temperature of 500° C. for 1 hr. Further, bismuth oxide fine particles and a boron oxide fine powder (whose average particle size is about 2 to 3 μm) were mixed at a weight ratio of 93:7. The mixed powder was heat treated at a temperature of 600° C. for 10 mins. These were blended at a weight ratio of 8:2 and ground fine to obtain a synthetic powder of bismuth oxide/antimony oxide/chromium oxide/boron oxide (whose average particle size is about 2 to 3 μm).

Workup

  1. temperatureThe mixed powder was heat
  2. additiontreated at a temperature of 500° C. for 1 hr
  3. temperatureThe mixed powder was heat
  4. additiontreated at a temperature of 600° C. for 10 mins

Sources & evidence

ORD record
ord-7864c291a7724a21b8e421655d891841
Source dataset
uspto-grants-1998_04
Patent number
US05739742

Reaction notes

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