huagongshe.com
HRID1599403

反应详情

EQUATION

反应方程式

HRID 1599403 的结构方程式

REACTANTS

反应物

2
结构：CCC(C)(CO)CO
HCID66169

2-Ethyl-2-methylpropane-1,3-diol

C6H14O2

结构：O=[N+]([O-])c1ccc(CP(=O)(O)O)cc1
HCID5180708

(4-Nitro-benzyl)-phosphonic acid

C7H8NO5P

PRODUCTS

生成物

1
结构：CCC1(C)COP(=O)(Cc2ccc([N+](=O)[O-])cc2)OC1
HCID18928069

未命名化合物

PROCEDURE

实验过程

With 4-nitrobenzylphosphonic acid and 2-ethyl-2-methyl-1,3-propanediol, the same procedure as in Reference Example 11 was followed, to yield 5-ethyl-5-methyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinane-2-oxide, which was then recrystallized from ethanol-hexane to yield colorless prisms having a melting point of 184° to 185° C.