HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 18920425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 3-Butyn-1-ol, 4-(5-(2-thienyl)-2-thienyl)- | HCID 440357 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18920425 | HCID 18920425 | — |
Reaction Steps
5-(4-Hydroxy-1-butynyl)-2,2'-bithiophene (0.8 g) was dissolved in pyridine (8 ml). Benzoyl chloride (1 ml) was added at room temperature, stirred for few minutes and kept overnight. The reaction mixture was treated as in example 21. Light yellowish crystals were then obtained and the melting point thereof was 61° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05741811 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-e298262f168f4b73a35db4fd73b01791 |
| Source note | uspto-grants-1998_04 |