HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Bis(aminomethyl)cyclohexane → 1,3-Benzenedimethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Bis(aminomethyl)cyclohexane | HCID 17406 | — |
| Solvent | M-Xylene | HCID 7929 | — |
| Product | 1,3-Benzenedimethanamine | HCID 15133 | — |
| Product | 3-Methylbenzylamine | HCID 66015 | — |
| Product | (3-Methylcyclohexyl)methanamine | HCID 18361468 | — |
Reaction Steps
As a result of analysis by gaschromatography, it was found that the yield of 1,3-bis(aminomethyl)cyclohexane was 94.0 mol %, and as other products 0.5 mol % of metaxylene, 3.7 mol % of 3-aminomethyl-1-methylcyclohexane, 1.7 mol % of 3-methylbenzylamine and 0.1 mol % of unreacted metaxylylenediamine were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05741928 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-d2a65e771ade496c8d8da8007f8fbd10 |
| Source note | uspto-grants-1998_04 |