HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Bis(aminomethyl)cyclohexane → 1,3-Benzenedimethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Bis(aminomethyl)cyclohexane | HCID 17406 | — |
| Solvent | M-Xylene | HCID 7929 | — |
| Product | 1,3-Benzenedimethanamine | HCID 15133 | — |
| Product | 3-Methylbenzylamine | HCID 66015 | — |
| Product | (3-Methylcyclohexyl)methanamine | HCID 18361468 | — |
Reaction Steps
As a result of analysis by gaschromatography, it was found that the yield of 1,3-bis(aminomethyl)cyclohexane was 91.5 mol %, and as other products 0.6 mol % of 3-aminomethyl-1-methylcyclohexane, 4.6 mol % of 3-methylbenzylamine, 0.2 mol % of metaxylene and 3.1 mol % of unreacted metaxylylenediamine were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05741928 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-3021576c3f134b63aab4d18f8d79e7e9 |
| Source note | uspto-grants-1998_04 |