2-(Ethylthio)ethanol → HCID 88265867, compound

HRID 1599965Notes

Reaction equation

HRID 1599965 reaction equation
[Na+].Cl[Au-:3](Cl)(Cl)Cl.OCCSCC.[SH:13][CH2:14][CH2:15][C:16]([NH:18][CH2:19][C:20]([OH:22])=[O:21])=[O:17]>O>[SH:13][CH2:14][CH2:15][C:16]([NH:18][CH2:19][C:20]([OH:22])=[O:21])=[O:17].[Au:3]

Participants

5

Reactant 3

HCID 80752-(Ethylthio)ethanolHCID 27127Sodium tetrachloroaurateHCID 165505N-(3-Mercapto-1-oxopropyl)glycine

Product 1

HCID 88265867HCID 88265867, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A solution of sodium tetrachloroaurate (35 g) in distilled water (200 ml) was slowly added to a solution of ethyl 2-hydroxyethyl sulphide (20.5 g) in distilled water (200 ml). Solid addition of mercaptopropionylglycine (5.21 g) followed by vigorous stirring yielded gold mercaptopropionylglycine as a white solid (yield, based on gold, 85%).

Workup

  1. customyielded

Sources & evidence

ORD record
ord-a6366187493e48cb9daf116ebdebe9b9
Source dataset
uspto-grants-1998_04
Patent number
US05744245

Reaction notes

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