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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1600103Generated: October 25, 2026

Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester → cis-(+/-)-5-(Azidomethyl)tetrahydro-3-furanthiol

https://huagongshe.com/reaction/1600103

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]esterHCID 86750331—
SolventTetrahydrofuranHCID 8028—
SolventSodium methanolate methanolHCID 23694274—
Productcis-(+/-)-5-(Azidomethyl)tetrahydro-3-furanthiolHCID 86750332—

Reaction Steps

The title compound is prepared by the procedure of Example 16 using 0.310 gof product from Example 61 in 4.5 ml of tetrahydrofuran and 0.30 ml of 25% sodium methoxide/methyl alcohol to give 0.159 g of the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05744465
Source datasetuspto-grants-1998_04
ORD IDord-5d5677a058ef40e5b221235ac4228555
Source noteuspto-grants-1998_04