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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1600112Generated: November 4, 2026

Water → HCID 86752474, compound

https://huagongshe.com/reaction/1600112

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 86750339HCID 86750339—
CatalystPalladiumHCID 23938—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 86752474HCID 86752474—

Reaction Steps

The title compound is prepared by the procedure of Example 18 using 0.387 gof product from Example 91, 0.046 g of sodium bicarbonate, 4 ml of water, 19 ml of dioxane, and 0.050 g of 10% palladium/carbon to give 0.031 g of the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05744465
Source datasetuspto-grants-1998_04
ORD IDord-3b134e4186404ab78d513f68e8e40559
Source noteuspto-grants-1998_04