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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1600114Generated: November 2, 2026

Water → HCID 86752476, compound

https://huagongshe.com/reaction/1600114

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 86752478HCID 86752478—
CatalystPalladiumHCID 23938—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 86752476HCID 86752476—

Reaction Steps

The title compound is prepared by the procedure of Example 18 using 0.150 gof product from Example 95, 0.025 g of sodium bicarbonate, 3 ml of water, 9ml of dioxane and 0.030 g of 10% palladium/carbon to give 0.0786 g of the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05744465
Source datasetuspto-grants-1998_04
ORD IDord-e31374fa044342d6a5d67c0d5048cf4f
Source noteuspto-grants-1998_04