HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → L-Valine, N-[[(4-nitrophenyl)methoxy]carbonyl]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | L-Valine | HCID 6287 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Carbonic acid 4-Nitrophenyl (4-Nitrophenyl)methyl Ester | HCID 21829967 | — |
| Solvent | Water | HCID 962 | — |
| Product | L-Valine, N-[[(4-nitrophenyl)methoxy]carbonyl]- | HCID 54494215 | 35.7% |
Reaction Steps
The title compound is prepared by the procedure of Example 255 using 14.73 g of product from Example 254, 5.42 g of L-valine, 12.75 ml of triethylamine and 556 ml of 4:1 ethyl alcohol:water to give 4.89 g of the desired product after chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744465 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-59c7c48f803547969d401d2a18112286 |
| Source note | uspto-grants-1998_04 |