HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 1-acetoxyethyl p-nitrophenyl carbonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 1-chloroethyl (4-nitrophenyl) Carbonate | HCID 10538354 | — |
| Product | 1-acetoxyethyl p-nitrophenyl carbonate | HCID 11780560 | — |
Reaction Steps
To a solution of 10.0 g of product from Example 317 in 250 ml of acetic acid is added 15.0 g mercuric acetate. The mixture is stirred at room temperature for 22 hours, concentrated in vacuo, and purified by chromatography (Silica gel: methylene chloride -5% methyl alcohol/methylene chloride) to give 7.5 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744465 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-08996550515543d2829925ed666e09bf |
| Source note | uspto-grants-1998_04 |