Ethyl Acetate → HCID 67618572, compound

Participants

Reaction Steps

A solution of 3-(4-fluorophenyl)propanal (7.0 g) in ether (50 ml) was addedto a stirred suspension of 4-nitrophenylhydrazine (7.0 g) in ether (1 50 ml), followed by sufficient ethyl acetate to achieve a clear solution. Thesolution was filtered and evaporated and the residue was crystallised from ethyl acetate/hexane to give the title compound (5.48 g), m.p. 125°-127° C. Found: C,62.81; H,4.87; N,14.44. C15 H14FN3O2 requires: C,62.71; H,4.91; N,14.63%.

Provenance & Evidence