Methyl iodide → HCID 19075471, compound

HRID 1600216Notes

Reaction equation

HRID 1600216 reaction equation
[CH3:1][I:2].[CH:3]([O:6][C:7]1[C:11]([C:12]2[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=2)=[N:10][S:9][N:8]=1)([CH3:5])[CH3:4]>CC(C)=O>[I-:2].[CH:3]([O:6][C:7]1[C:11]([C:12]2[CH:13]=[N+:14]([CH3:1])[CH:15]=[CH:16][CH:17]=2)=[N:10][S:9][N:8]=1)([CH3:5])[CH3:4]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19016549HCID 19016549, compound

Product 1

HCID 19075471HCID 19075471, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.3 ml, 5 mmol) and 3-(3-isopropoxy-1,2,5-thiadiazol-4-yl)pyridine (540 mg, 2.4 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration toyield 0.68 g (77%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration toyield 0.68 g (77%)

Sources & evidence

ORD record
ord-3610eaa096164e5cb7336b594de41991
Source dataset
uspto-grants-1998_04
Patent number
US05744489

Reaction notes

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