Methyl iodide → HCID 19075414, compound

HRID 1600220Notes

Reaction equation

HRID 1600220 reaction equation
[CH3:1][I:2].[CH2:3]([O:7][C:8]1[C:12]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:11][S:10][N:9]=1)[CH:4]([CH3:6])[CH3:5]>CC(C)=O>[I-:2].[CH2:3]([O:7][C:8]1[C:12]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:11][S:10][N:9]=1)[CH:4]([CH3:6])[CH3:5]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075496HCID 19075496, compound

Product 1

HCID 19075414HCID 19075414, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.6 ml, 10 mmol) and 3-(3-isobutoxy-1,2,5-thiadiazol-4-yl)pyridine (588 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration toyield 0.88 g (87%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration toyield 0.88 g (87%)

Sources & evidence

ORD record
ord-cd174bc968f84c85a1d60e565b3b6db6
Source dataset
uspto-grants-1998_04
Patent number
US05744489

Reaction notes

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