Methyl iodide → HCID 19075363, compound

HRID 1600222Notes

Reaction equation

HRID 1600222 reaction equation
[CH3:1][I:2].[CH2:3]([O:8][C:9]1[C:13]([C:14]2[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=2)=[N:12][S:11][N:10]=1)[CH2:4][CH:5]([CH3:7])[CH3:6]>CC(C)=O>[I-:2].[CH2:3]([O:8][C:9]1[C:13]([C:14]2[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=2)=[N:12][S:11][N:10]=1)[CH2:4][CH:5]([CH3:7])[CH3:6]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075319HCID 19075319, compound

Product 1

HCID 19075363HCID 19075363, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 10 mmol) and 3-(3-isopentyloxy-1,2,5-thiadiazol-4-yl)pyridine (622 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration toyield 0.78 g (81%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration toyield 0.78 g (81%)

Sources & evidence

ORD record
ord-ef6f38f01df14a6785f7924d0d3c126d
Source dataset
uspto-grants-1998_04
Patent number
US05744489

Reaction notes

Loading…