Methyl iodide → 3-(3-(2-(2-Butoxyethoxy) ethoxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

HRID 1600277Notes

Reaction equation

HRID 1600277 reaction equation
[CH3:1][I:2].[CH2:3]([O:7][CH2:8][CH2:9][O:10][CH2:11][CH2:12][O:13][C:14]1[C:18]([C:19]2[CH:20]=[N:21][CH:22]=[CH:23][CH:24]=2)=[N:17][S:16][N:15]=1)[CH2:4][CH2:5][CH3:6]>>[I-:2].[CH2:3]([O:7][CH2:8][CH2:9][O:10][CH2:11][CH2:12][O:13][C:14]1[C:18]([C:19]2[CH:20]=[N+:21]([CH3:1])[CH:22]=[CH:23][CH:24]=2)=[N:17][S:16][N:15]=1)[CH2:4][CH2:5][CH3:6]

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 190753243-(3-(2-(2-Butoxyethoxy)ethoxy)-1,2,5-thiadiazol-4-yl)pyridine

Product 1

HCID 190752543-(3-(2-(2-Butoxyethoxy) ethoxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

Procedure

A mixture of methyl iodide (0.5 ml, 9 mmol) and 3-(3-(2-(2-butoxyethoxy)ethoxy)-1,2,5-thiadiazol-4-yl)pyridine (3 mmol) inacetone (5 ml) was stirred at room temperature for 18 h. The title compoundprecipitated from the solution and was collected by filtration.

Workup

  1. filtrationwas collected by filtration

Sources & evidence

ORD record
ord-5b37e0d355bb42d597512fa44bced40a
Source dataset
uspto-grants-1998_04
Patent number
US05744489

Reaction notes

Loading…