Methyl iodide → 3-(4-(2-(2-Ethoxyethoxy)ethoxy)-1,2,5-thiadiazol-3-yl)-1-methylpyridinium iodide

HRID 1600279Notes

Reaction equation

HRID 1600279 reaction equation
[CH3:1][I:2].[CH2:3]([O:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10][O:11][C:12]1[C:16]([C:17]2[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=2)=[N:15][S:14][N:13]=1)[CH3:4]>>[I-:2].[CH2:3]([O:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10][O:11][C:12]1[C:16]([C:17]2[CH:18]=[N+:19]([CH3:1])[CH:20]=[CH:21][CH:22]=2)=[N:15][S:14][N:13]=1)[CH3:4]

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 190754773-(3-(2-(2-Ethoxyethoxy)ethoxy)-1,2,5-thiadiazol-4-yl)pyridine

Product 1

HCID 190753263-(4-(2-(2-Ethoxyethoxy)ethoxy)-1,2,5-thiadiazol-3-yl)-1-methylpyridinium iodide

Procedure

A mixture of methyl iodide (0.5 ml, 9 mmol) and 3-(3-(2-(2-ethoxyethoxy)ethoxy)-1,2,5-thiadiazol-4-yl)pyridine (3 mmol) inacetone (5 ml) was stirred at room temperature for 18 h. The title compoundprecipitated from the solution and was collected by filtration.

Workup

  1. filtrationwas collected by filtration

Sources & evidence

ORD record
ord-2ccbb4f359c14e789bbb13ff46c3e9a9
Source dataset
uspto-grants-1998_04
Patent number
US05744489

Reaction notes

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