Methyl iodide → HCID 19075355, compound

HRID 1600283Notes

Reaction equation

HRID 1600283 reaction equation
[CH3:1][I:2].[O:3]1[CH2:8][CH2:7][N:6]([C:9]2[C:13]([C:14]3[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=3)=[N:12][S:11][N:10]=2)[CH2:5][CH2:4]1>CC(C)=O>[I-:2].[O:3]1[CH2:4][CH2:5][N:6]([C:9]2[C:13]([C:14]3[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=3)=[N:12][S:11][N:10]=2)[CH2:7][CH2:8]1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075225HCID 19075225, compound

Product 1

HCID 19075355HCID 19075355, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 8 mmol) and 3-(3-morpholino-1,2,5-thiadiazol-4-yl)pyridine (680 mg, 2.7 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration toyield 1.0 g (94%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration toyield 1.0 g (94%)

Sources & evidence

ORD record
ord-8260629565bc44a5a7bf23a0eec8e94c
Source dataset
uspto-grants-1998_04
Patent number
US05744489

Reaction notes

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