Methyl iodide → HCID 19075210, compound

HRID 1600285Notes

Reaction equation

HRID 1600285 reaction equation
[CH3:1][I:2].[CH2:3]([NH:9][C:10]1[C:14]([C:15]2[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=2)=[N:13][S:12][N:11]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]>CC(C)=O>[I-:2].[CH2:3]([NH:9][C:10]1[C:14]([C:15]2[CH:16]=[N+:17]([CH3:1])[CH:18]=[CH:19][CH:20]=2)=[N:13][S:12][N:11]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180169HCID 15180169, compound

Product 1

HCID 19075210HCID 19075210, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.6 ml, 9.6 mmol) and 3-(3-hexylamino-1,2,5-thiadiazol-4-yl)pyridine (3.2 mmol) in acetone (5 ml) was stirred at room temperature for 18 h and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-67073ed8398b4f059ee1fb2f5be7902f
Source dataset
uspto-grants-1998_04
Patent number
US05744489

Reaction notes

Loading…