Methyl iodide → HCID 19075251, compound

HRID 1600287Notes

Reaction equation

HRID 1600287 reaction equation
[CH3:1][I:2].[CH2:3]([S:6][C:7]1[C:11]([C:12]2[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=2)=[N:10][S:9][N:8]=1)[CH2:4][CH3:5]>CC(C)=O>[I-:2].[CH2:3]([S:6][C:7]1[C:11]([C:12]2[CH:13]=[N+:14]([CH3:1])[CH:15]=[CH:16][CH:17]=2)=[N:10][S:9][N:8]=1)[CH2:4][CH3:5]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180155HCID 15180155, compound

Product 1

HCID 19075251HCID 19075251, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 8 mmol) and 3-(3-propylthio-1,2,-5-thiadiazol-4-yl)pyridine (0.63 g, 2.6 mmol) in acetone (5 ml) was stirred at room temperature for 18 h and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-c0ae1f52b6b14cd7a65dd5028a079342
Source dataset
uspto-grants-1998_04
Patent number
US05744489

Reaction notes

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