Methyl iodide → HCID 19075272, compound

HRID 1600307Notes

Reaction equation

HRID 1600307 reaction equation
[CH3:1][I:2].[CH2:3]([S:8][C:9]1[C:13]([C:14]2[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=2)=[N:12][S:11][N:10]=1)[CH2:4][CH2:5][CH2:6][CH3:7]>>[I-:2].[CH2:3]([S:8][C:9]1[C:13]([C:14]2[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=2)=[N:12][S:11][N:10]=1)[CH2:4][CH2:5][CH2:6][CH3:7]

Participants

3

Procedure

Methyl iodide (0.5 ml, 7.5 mmol) was added to a solution of 3-(3-pentylthio-1,2,5-thiadiazol-4-yl)pyridine (3 mmol) and the reaction mixture was stirred at room temperature for 48 h and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-9403844bb7c3484da8ddcc73c9bc661e
Source dataset
uspto-grants-1998_04
Patent number
US05744489

Reaction notes

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