HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → Boc-D-alanine Ethyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | BOC-D-alanine | HCID 637606 | — |
| Product | Boc-D-alanine Ethyl Ester | HCID 12515028 | 48.8% |
Reaction Steps
The title compound was prepared by the method of Example 8 using ethyl iodide (2.4 mL, 30 mmol) instead of methyl iodide and BOC-D-Ala-OH (5.0 g,26.4 mmol) instead of the product of Example 1. Concentration afforded the title compound (2.8 g) as a pale yellow oil and the structure verified by NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744631 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-f77338553cb94f15acfed47967885739 |
| Source note | uspto-grants-1998_04 |