Methyl iodide → HCID 19612631, compound

HRID 1600459Notes

Reaction equation

HRID 1600459 reaction equation
[CH3:1][I:2].[C:3]1([CH2:9][CH2:10][CH2:11][S:12][C:13]2[C:17]([C:18]3[CH:19]=[N:20][CH:21]=[CH:22][CH:23]=3)=[N:16][O:15][N:14]=2)[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>CC(C)=O>[I-:2].[C:3]1([CH2:9][CH2:10][CH2:11][S:12][C:13]2[C:17]([C:18]3[CH:19]=[N+:20]([CH3:1])[CH:21]=[CH:22][CH:23]=3)=[N:16][O:15][N:14]=2)[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

Participants

4

Procedure

Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(3-(3-phenylpropylthio)-1,2,5-oxadiazol-4-yl)pyridine (7 mmol) in acetone and the reaction mixture was stirred at room temperature for 20 h. and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-5334e7ace7cb4bdd8f4bc70666ccc132
Source dataset
uspto-grants-1999_11
Patent number
USRE036375

Reaction notes

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