Benzylamine → HCID 19613971, compound

HRID 1600465Notes

Reaction equation

HRID 1600465 reaction equation
C([O:4][C:5]1[CH:10]=[CH:9][C:8]([C:11]([O:13][CH:14]([CH2:17][CH3:18])[CH2:15][CH3:16])=[O:12])=[C:7]([F:19])[CH:6]=1)(=O)C.C(N)C1C=CC=CC=1>C(O)C.CCOCC>[OH:4][C:5]1[CH:10]=[CH:9][C:8]([C:11]([O:13][CH:14]([CH2:17][CH3:18])[CH2:15][CH3:16])=[O:12])=[C:7]([F:19])[CH:6]=1

Participants

5

Reactant 2

HCID 7504BenzylamineHCID 19613967HCID 19613967, compound

Product 1

HCID 19613971HCID 19613971, compound

Reagents, catalysts & solvents 2

HCID 702EthanolSolventHCID 3283Diethyl EtherSolvent

Procedure

0.5 Gram of the compound obtained in the above (3) was dissolved in 30 ml of ethanol, and 1.5 g of benzylamine was added dropwise thereto. Further, the mixture was stirred at room temperature for one day and diluted with 300 ml of ether, and the diluted mixture was washed with diluted hydrochloric acid and then with water and dried over magnesium sulfate.

Workup

  1. washthe diluted mixture was washed with diluted hydrochloric acid
  2. dry with materialwith water and dried over magnesium sulfate

Sources & evidence

ORD record
ord-8eb39357567449b8b708235f99951a97
Source dataset
uspto-grants-1999_11
Patent number
US05976409

Reaction notes

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