Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methacrylamide | HCID 6595 | — |
| Reactant | Glycidyl methacrylate | HCID 7837 | — |
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | 4,4-Azobis(4-cyanovaleric acid) | HCID 92938 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Water | HCID 962 | — |
| Product | Isobutyl Methacrylate | HCID 7352 | — |
Reaction Steps
is added within 3 hours at 80° C. Thereafter a solution of 10 g of methacrylamide and 0.6 g of the sodium salt of 4,4'-azobis-(4-cyanovaleric acid) in 300 ml of water and a monomer mixture consisting of 50 g of ethyl acrylate and 45 g of glycidyl methacrylate are added simultaneously. After stirring for 60 minutes at 80° C. one obtains a coagulate-free dispersion with a solid content of 20%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05976527 |
|---|
| Source dataset | uspto-grants-1999_11 |
|---|
| ORD ID | ord-59542dc8c54c4e60a4d275ff50136a75 |
|---|
| Source note | uspto-grants-1999_11 |
|---|
