HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl vinyl ether → p-1-Ethoxyethoxystyrene p-hydroxystyrene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl vinyl ether | HCID 8023 | — |
| Reactant | 4-Ethynylphenol | HCID 32758 | — |
| Product | p-1-Ethoxyethoxystyrene p-hydroxystyrene | HCID 131719558 | — |
Reaction Steps
Using 16.0 g of poly(p-hydroxystyrene) obtained according to (2) of Preparation Example 10 and 4.5 g of vinylethyl ether, the procedure of (3) of Preparation Example 1 was carried out to obtain 15.5 g of poly(p-1-ethoxyethoxystyrene/p-hydroxystyrene). P-1-ethoxyethoxystyrene unit/p-hydroxystyrene unit molar ratio in the polymer≈38:62. Mw≈9,500; Mw/Mn=1.65 (GPC with polystyrene calibration).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05976759 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-a9849b1404f24ffebb77724df915aaeb |
| Source note | uspto-grants-1999_11 |