Isopropyl chloroformate → HCID 86754732, compound

Participants

Reaction Steps

Using 12.0 g of poly(p-hydroxystyrene) obtained according to (2) above and 3.0 g of isopropyl chlorocarbonate, reaction and after-treatments were carried out according to (2) of Preparation Example 6 to obtain 11.7 g of poly(p-isopropoxycarbonyloxystyrene/p-hydroxystyrene) as white powdery crystal. P-isopropoxycarbonyloxystyrene unit/p-hydorxystyrene unit molar ratio in the polymer≈2:8 (1H NMR). Mw≈8,000; Mw/Mn=1.60 (GPC with polystyrene calibration).

Provenance & Evidence