HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → benzyl 2-(N-methyleneamino)-2-methylpropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Benzyl 2-amino-2-methylbutyrate | HCID 21829894 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | benzyl 2-(N-methyleneamino)-2-methylpropanoate | HCID 19354575 | 106.7% |
Reaction Steps
To benzyl 2-amino-2-methylbutyrate (12.96 g) was dropped at room temperature 37% formalin (7.62 g), and the mixture was stirred for 4 h. The reaction mixture was dissolved in ether and washed with water. The organic phase was dried over magnesium sulfate, filtered and evaporated to get the captioned compound (13.7 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977025 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-670e81ef862144a281e4a9bd8d1a1375 |
| Source note | uspto-grants-1999_11 |