HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl vinyl ketone → HCID 21829922, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl vinyl ketone | HCID 6570 | — |
| Reactant | HCID 21829902 | HCID 21829902 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21829922 | HCID 21829922 | 97.4% |
Reaction Steps
Methyl vinyl ketone (1.02 g) was added to a solution of N-(2,5-dichlorophenyl)-2-aminoisobutyramide (2.4 g) in tetrahydrofuran (10 mL) and the mixture was heated at reflux 30 hours. After distilling off the solvent under reduced pressure, 3 g of N-(2,5-dichlorophenyl)-2-(3-oxobutylamino)isobutyramide was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977027 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-88f9a1e684d14fed93cc8ab79e568b4b |
| Source note | uspto-grants-1999_11 |