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HRID1600881

反应详情

EQUATION

反应方程式

HRID 1600881 的结构方程式

REACTANTS

反应物

2
结构：Clc1ccc2cc[nH]c2n1
HCID11344118

6-Chloro-7-azaindole

C7H5ClN2

结构：CN(C)CC(=O)Cl.Cl
HCID13994991

N,N-Dimethylglycyl chloride--hydrogen chloride (1/1)

C4H9Cl2NO

PRODUCTS

生成物

1
结构：CN(C)CC(=O)c1cn(Cl)c2ncccc12
HCID86754739

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 6-chloro-1H-pyrrolo[2,3-b]pyridine (Synthesis, 992, 7, 661-663) and dimethylaminoacetyl chloride hydrochloride (Arch. Pharm. 991, 324, 433-437) in a procedure similar to Example 1. NMR (D6DMSO) δ8 12.65 (s, 1H), 8.60 (s, 1H), 7.95 (d, 1H), 7.32 (d, 1H), 3.60 (s, 2H), 2.22 (s, 3H). 13C NMR (D6DMSO) 195.6, 147.5, 144.4, 134.8, 132.7, 118.0, 116.8, 114.0, 65.9, 45,4 (2). Mass spectrum: 237,239 (P+1, P+3).