HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → (+/-)-alpha-(4-Phenylphenylthiomethyl)-3-pyridinepropanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 4-Phenylbenzene-1-thiol | HCID 2760414 | — |
| Reactant | HCID 10877288 | HCID 10877288 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | (+/-)-alpha-(4-Phenylphenylthiomethyl)-3-pyridinepropanol | HCID 21830749 | 29.9% |
Reaction Steps
Prepared according to the method described in Example 1 from 4-phenylthiophenol (0.186 g), sodium hydride (0.044 g) and (±)-3-(2-oxiranylethyl)pyridine (0.150 g) in dimethylformamide (3 ml) at room temperature to give the title compound as a solid (0.100 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977105 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-8b57fc36fb654ba5aa66406c90472b94 |
| Source note | uspto-grants-1999_11 |