HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18394403, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 2,3-Dimethylaniline | HCID 6893 | — |
| Reactant | (3S)-2-((tert-butoxy)carbonyl)-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid | HCID 664088 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18394403 | HCID 18394403 | — |
Reaction Steps
N-Boc-L-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid (Bachem) was coupled with 2,3-dimethyl aniline using standard peptide coupling procedures. The product was deprotected using TFA in CH2Cl2 to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977134 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-061bcb8e2a53406590aada6e06fba8de |
| Source note | uspto-grants-1999_11 |