HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminobenzoic Acid → Ethyl 3-[4-(carboxy)phenylamino]propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminobenzoic Acid | HCID 978 | — |
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Ethyl 3-[4-(carboxy)phenylamino]propionate | HCID 21830455 | 63.2% |
Reaction Steps
A solution of 4-aminobenzoic acid (6.85 g, 0.05 mol) and ethyl acrylate (15 g, 0.15 mol) in acetic acid (40 mL) was heated to 100° C. for 15 h. The solid which formed was filtered, washed with hexane and dried to give of the title compound (7.5 g, 63%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977101 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-bbf67556227a467e930b816c8786da9a |
| Source note | uspto-grants-1999_11 |