HCID 54135925, compound → HCID 54042444, compound

Participants

Reaction Steps

Following the procedure of Example 82(e), except substituting dimethyl 4-[2-(Cbz-methylamino)acetyl]-1,2-phenylenedioxydiacetate (2.1 g, 4.57 mmol) for benzyl 4-[2-[[[1-[(benzimidazol-2-yl)methyl]benzimidazol-2-yl]methyl]methylamino]acetyl]-phenoxyacetate and using EtOAc (50 mL) and MeOH (20 mL) as solvents, the title compound (1.34 g, 90%) was prepared: MS (ES) m/e 328.0 [M+H]+.

Provenance & Evidence