HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-((2-(2,4-Difluorophenyl)-3-methyloxiran-2-yl)methyl)-1H-1,2,4-triazole, (2R-cis)- → HCID 178462410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-((2-(2,4-Difluorophenyl)-3-methyloxiran-2-yl)methyl)-1H-1,2,4-triazole, (2R-cis)- | HCID 10131191 | — |
| Reactant | HCID 178477154 | HCID 178477154 | — |
| Product | HCID 178462410 | HCID 178462410 | 70% |
Reaction Steps
Reaction and treatment were carried out in the same manner as in Example 1 using (2R,3S)-2-(2,4-difluorophenyl)-3-methyl-2-[(1H-1,2,4-triazol-1-yl)methyl]oxirane and trans-5-(acetylthio)-2-[(E)-2-[4-(trifluoromethyl)phenyl]vinyl]-1,3-dioxane to obtain the desired compound having a melting point of 73 to 75° C. in a yield of 70%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977152 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-9e5f8a69d87b404789031debeb3864b8 |
| Source note | uspto-grants-1999_11 |