HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 21832301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 2-Chlorobenzoyl chloride | HCID 69110 | — |
| Reactant | HCID 11746174 | HCID 11746174 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 21832301 | HCID 21832301 | — |
Reaction Steps
A tetrahydrofuran (5 ml) solution of 2-chlorobenzoyl chloride (0.88 g) was added dropwise under ice-cooling and stirring to a tetrahydrofuran (20 ml) solution of 2-(4-trifluoromethoxyphenoxy)ethylamine (1.10 g) and triethylamine (0.51 g) and the mixture was further stirred at room temperature for one hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977410 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-6c229dca8ee9488aa5971163921b9928 |
| Source note | uspto-grants-1999_11 |