HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 21832298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 2,6-Difluorobenzoyl chloride | HCID 87438 | — |
| Reactant | HCID 21832286 | HCID 21832286 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 21832298 | HCID 21832298 | — |
Reaction Steps
A tetrahydrofuran (5 ml) solution of 2,6-difluorobenzoyl chloride (0.71 g) was added dropwise under ice-cooling and stirring to a tetrahydrofuran (20 ml) solution of 2-[4-(2-chloro-1,1,2-trifluoroethoxy)phenoxy]ethylamine (1.08 g) and triethylamine (0.40 g) and the mixture was further stirred at room temperature for one hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977410 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-3aece8d04973433bba95f57f12ee427e |
| Source note | uspto-grants-1999_11 |