Lawesson's reagent → HCID 21832302, compound

HRID 1601756Notes

Reaction equation

HRID 1601756 reaction equation
COC1C=CC(P2(SP(C3C=CC(OC)=CC=3)(=S)S2)=[S:10])=CC=1.[F:23][C:24]([F:47])([F:46])[O:25][C:26]1[CH:45]=[CH:44][C:29]([O:30][CH2:31][CH2:32][NH:33][C:34](=O)[C:35]2[C:40]([F:41])=[CH:39][CH:38]=[CH:37][C:36]=2[F:42])=[CH:28][CH:27]=1>C1(C)C=CC=CC=1>[F:23][C:24]([F:47])([F:46])[O:25][C:26]1[CH:45]=[CH:44][C:29]([O:30][CH2:31][CH2:32][NH:33][C:34](=[S:10])[C:35]2[C:40]([F:41])=[CH:39][CH:38]=[CH:37][C:36]=2[F:42])=[CH:28][CH:27]=1

Participants

4

Reactant 2

HCID 87949Lawesson's reagentHCID 21832291HCID 21832291, compound

Product 1

HCID 21832302HCID 21832302, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Lawesson's reagent (1.94 g) was added to a toluene (20 ml) solution of N-[2-(4-trifluoromethoxyphenoxy)ethyl]-2,6-difluorobenzamide (1.44 g) and the mixture was stirred at room temperature for 3 hours.

Sources & evidence

ORD record
ord-06d6acd0e5274d57bdd22364def7ce77
Source dataset
uspto-grants-1999_11
Patent number
US05977410

Reaction notes

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