Acetic Acid → HCID 21832000, compound

Participants

Reaction Steps

A procedure similar to that described in Example 12 was repeated, except that 3.40 g of 5-{4-(1-methyl-1H-imidazo[4,5-c]pyridin-2-ylmethoxy)benzyl}-3-triphenylmethylthiazolidine-2,4-dione (prepared as described in Preparation 74) and 24 ml of a 3:1 by volume mixture of acetic acid and water were used, to give the title compound as a crude product. This crude product was crystallized by trituration with ethyl acetate, to give 1.01 g of the title compound, melting at 264-265° C.

Provenance & Evidence